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. 2003 Jun 10;100(13):7913–7918. doi: 10.1073/pnas.1232451100

Table 3. Coupling constants (J, Hz) of galactopyranose and glycerol residues of glycolipid derivatives and related reference compounds.

	BbGL-I CDCl₃	BbGL-I-Ac₃ CDCl₃	BbGL-II CDCl₃	BbGL-II-Ac₄ CDCl₃	MGDG CDCl₃:CD₃OD^*	1,2-Dipalmitin CDCl₃	Me-α-d-Galp D₂O	Me-β-d-Galp D₂O
J_1′,2′ (Gal)	7.5	8.0	3.8	3.7	7.3		3.4	8.0
J_2′,3′	ND	10.5	9.8	10.0	9.7		10.1	9.9
J_3′,4′	3.2^†	3.5	3.2	3.5	3.3		2.8	3.5
J_4′,5′	1.0^†	1.0	1.1	1.1	1.1		1.6	0.8
J_5′,6′a	6.3	6.7	5.1	6.4	6.5		6.8	7.9
J_5′,6′b	7.2	6.7	ND	7.0	5.4		5.5	4.4
J_6′a,6′b	11.1	11.2	11.5	11.2	11.6		11.7	11.7
¹J_{C-1′,H-1′}	158.7	157.4	170.5	172.4	160.2		170.2	160.6
J_{1″″a,1″″b} (Gro)			11.9	11.8	12.1	11.9
J_{1″″a,2″″}			4.1	4.1	3.2	4.5
J_{1″″b,2″″}			5.9	6.1	6.7	5.7
J_{2″″,3″″a}			4.8	4.3	5.4	4.8
J_{2″″,3″″b}			6.2	5.2	6.0	5.2
J_{3″″a,3″″b}			10.9	11.2	10.9	12.2

ND, not determined

^*

4:1 vol/vol

^†

In (CD₃)₂CO:CDCl₃ (7:3 vol/vol) solution