TABLE 1.
Chemical shifts and scalar coupling constants of peptide 1-25 measured in 95% methanol solution
| Residue | NH | Hα | Hβ | Hγ | Hδ | Other | 3JΦa |
|---|---|---|---|---|---|---|---|
| 1A | 4.3 | 1.56 | b | ||||
| 2K | 8.56 | 4.43 | 1.74-1.89 | 1.47-1.53 | 1.72 | 2.97 | b |
| 3V | 8.05 | 3.73 | 2.08 | 0.89-0.97 | 7.7 | ||
| 4N | 8.57 | 4.83 | 2.64-2.70 | 7.07-7.73 | b | ||
| 5I | 8.25 | 4.4 | 2.13 | 1.35-1.49 | 0.99 | 1 | 7.9 |
| 6K | 8.53 | 4.3 | 1.95-2.09 | 1.56 | 1.68-1.81 | 3 | 2.8 |
| 7P | 4.43 | 2.10-2.35 | 1.81-1.94 | 3.65 | |||
| 8L | 7.18 | 4.15 | 1.74-1.86 | 0.90-0.97 | 4.5 | ||
| 9E | 8.09 | 4.02 | 2.15-2.28 | 2.43-2.52 | 3.2 | ||
| 10D | 8.76 | 4.41 | 2.61-2.91 | <3 | |||
| 11K | 7.81 | 3.95 | 2.06-2.10 | 1.32 | 1.52-1.67 | 2.96 | b |
| 12I | 8.04 | 4.19 | 2.04 | 1.16-1.29 | 0.9 | <3 | |
| 13L | 8.25 | 4.09 | 1.88-1.96 | 1.68 | 0.92-0.98 | <3 | |
| 14V | 8.3 | 3.73 | 2.25 | 0.97-1.15 | 3.4 | ||
| 15Q | 8.38 | 4.06 | 2.16-2.36 | 2.59-2.61 | 6.82-7.54 | 2.8 | |
| 16A | 8.81 | 4.11 | 1.55 | <3 | |||
| 17N | 8.4 | 4.51 | 2.81-3.00 | 6.88-7.60 | 4.2 | ||
| 18E | 8.69 | 4.12 | 2.10-2.37 | 2.42-2.72 | <3 | ||
| 19A | 8.56 | 4.15 | 1.58 | <3 | |||
| 20E | 8.38 | 4.18 | 2.24-2.33 | 2.51-2.66 | 3.0 | ||
| 21T | 8.12 | 4.12 | 4.33 | 1.3 | 4.5 | ||
| 22T | 7.94 | 4.43 | 4.43 | 1.48 | 3.1 | ||
| 23T | 7.93 | 4.21 | 4.34 | 3.2 | |||
| 24A | 7.77 | 4.31 | 1.28 | b | |||
| 25S | 7.8 | 4.5 | 3.93-3.96 | b |
a
b, broad.