Skip to main content
. 2003 Aug;69(8):4706–4713. doi: 10.1128/AEM.69.8.4706-4713.2003

TABLE 4.

NMR data for photobactin

Positiona δC δH, multiplicity, J (Hz) HMBCb
1 150.3
2 147.3
3 119.56 or 119.52 6.91, dd, 8.0, 1.5 C-1, C-5
4 119.56 or 119.52 6.69, t, 8.0 C-2, C-6
5 118.6 7.18, dd, 8.0, 1.5 C-1, C-3, C-7
6 116.7
7 171.5
9 40.13 or 40.06 3.38, br t, 6.5 C-7, C-10 or C-11
10 27.79 or 27.75 1.61, m C-11
11 27.79 or 27.75 1.61, m C-10
12 40.13 or 40.06 3.28, br t, 6.5 C-10 or C-110, C-14
14 172.9
15 75.8 4.41, d, 7.5 C-14, C-16, C-17, C-24
16 80.7 4.86, dd, 7.5, 6.5 C-14, C-17
17 168.4
18 111.8
19 149.5
20 146.7
21 120.3 6.94, dd, 8.0, 1.5 C-19, C-24
22 119.92 or 119.87 6.72, t, 8.0 C-18, C-20
23 119.92 or 119.87 7.15, dd, 8.0, 1.5 C-17, C-19, C-21
24 21.3 1.51, t, 6.5 C-15, C-16
a

Position as indicated in Fig. 4A.

b

HMBC, heteronuclear multibond conductivity.