TABLE 4.
Positiona | δC | δH, multiplicity, J (Hz) | HMBCb |
---|---|---|---|
1 | 150.3 | ||
2 | 147.3 | ||
3 | 119.56 or 119.52 | 6.91, dd, 8.0, 1.5 | C-1, C-5 |
4 | 119.56 or 119.52 | 6.69, t, 8.0 | C-2, C-6 |
5 | 118.6 | 7.18, dd, 8.0, 1.5 | C-1, C-3, C-7 |
6 | 116.7 | ||
7 | 171.5 | ||
9 | 40.13 or 40.06 | 3.38, br t, 6.5 | C-7, C-10 or C-11 |
10 | 27.79 or 27.75 | 1.61, m | C-11 |
11 | 27.79 or 27.75 | 1.61, m | C-10 |
12 | 40.13 or 40.06 | 3.28, br t, 6.5 | C-10 or C-110, C-14 |
14 | 172.9 | ||
15 | 75.8 | 4.41, d, 7.5 | C-14, C-16, C-17, C-24 |
16 | 80.7 | 4.86, dd, 7.5, 6.5 | C-14, C-17 |
17 | 168.4 | ||
18 | 111.8 | ||
19 | 149.5 | ||
20 | 146.7 | ||
21 | 120.3 | 6.94, dd, 8.0, 1.5 | C-19, C-24 |
22 | 119.92 or 119.87 | 6.72, t, 8.0 | C-18, C-20 |
23 | 119.92 or 119.87 | 7.15, dd, 8.0, 1.5 | C-17, C-19, C-21 |
24 | 21.3 | 1.51, t, 6.5 | C-15, C-16 |
Position as indicated in Fig. 4A.
HMBC, heteronuclear multibond conductivity.