Table 1.
Data collection statistics
| Data set | RC1 | RC2 | HiPIP |
| X-ray source | BL-6A(PF) | BL-41XU(SPring-8) | BL-6A(PF) |
| Wavelength (Å) | 1.000 | 0.708 | 1.000 |
| Temperature (K) | Ambient | 100 | Ambient |
| Resolution limits (Å) | 20–2.5 | 20–2.2 | 20–1.5 |
| Highest-resolution shell (Å) | 2.56–2.5 | 2.25–2.2 | 1.53–1.5 |
| Space group | P212121 | P212121 | P212121 |
| Unit cell dimensions (Å) | 134.2, 200.6, 85.0 | 133.3, 196.6, 84.2 | 47.2, 59.6, 23.6 |
| Measured reflections | 245,871 | 508,729 | 50,767 |
| Unique reflections | 63,727 | 110,923 | 10,306 |
| Rmerge (%)* | 7.7 (39.2) | 9.3 (36.2) | 6.7 (21.9) |
| Completeness (%)* | 80.3 (55.5) | 92.6 (78.6) | 86.7 (67.6) |
| l/σ(l)* | 9.4 (2.9) | 12.6 (2.6) | 13.1 (6.0) |
*
The value for the highest resolution shell in parenthesis.