Table 1. Data collection and refinement.
Numbers in parentheses for data collection refer to the highest resolution shell.
| Parameter | Value | |
|---|---|---|
| Data collection | ||
| Space group | C2 | P212121 |
| Unit cell [a, b, c (Å), β (°)] | 62.2, 31.1, 81.9, 102.2 | 36.3, 62.1, 67.5, 90.0 |
| Resolution range (Å) | 30.63-2.10 (2.21–2.10) | 20.72-1.50 (1.58–1.50) |
| Number of unique observations | 8653 (1180) | 24972 (3424) |
| Number of total observations | 43169 (5102) | 217987 (14791) |
| Completeness (%) | 95.1 (89.9) | 99.3 (95.6) |
| Multiplicity | 5.0 (4.3) | 8.7 (4.3) |
| Rmerge (%) | 6.8 (22.1) | 6.0 (33.7) |
| 〈I/σ(I)〉 | 16.9 (5.6) | 24.8 (2.7) |
| Refinement | ||
| R factor (%) | 16.3 | 15.0 |
| Rfree (%) | 22.5 | 21.4 |
| Rmsd bond length (Å) [angle (°)] | 0.014 (1.53) | 0.011 (1.47) |
| PDB code | 2BMJ | 2IWR |