Table 1.

Summary of crystallographic data and refinement statistics

	M184I RT/DNA/Fab		M184I RT, unliganded
Space group	P3212	P3212	C2
Temperature, °C	−10	−165	−165
Resolution range, Å	40−3.5	40−3.6	40−2.85
Cell parameters, a, Å	169.2	167.4	238.6
b, Å	169.2	167.4	72.7
c, Å	221.9	219.7	95.3
β, °	90	90	105.6
Completeness, %	91.5 (83)	84.0 (82)	94.9 (88)
(highest shell)
Rmerge, %	11.8	11.3	9.0
Refinement statistics
Resolution range, Å	10−3.5		8−2.85
No. of reflections	39,033		31,200
R-factor	26.2		25.9
Free R-factor	33.8		34.6
No. of protein atoms	11,720		7,700
Luzzati error, Å	0.53		0.48