| Data collection | |
| Bruker SMART 1000 CCD | 4996 independent reflections |
| diffractometer | 3117 reflections with I > 2σ(I) |
| thin–slice ω scans | Rint = 0.095 |
| Absorption correction: none | θmax = 23.3° |
| 26495 measured reflections |
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