Table 1.
O-Octyl | Glc | Man' | GlcNAc” | Distance(Å) |
---|---|---|---|---|
CH2-1b | H1 | --- | --- | 3.0 |
CH2-1a | H1 | --- | --- | 3.0 |
CH2-2 | H1 | --- | --- | 3.5 |
--- | H5 - H6(S) | --- | --- | 2.2 |
--- | H1 - H6(S) | --- | --- | 3.3 |
--- | H6(S) | H1' | --- | 2.5 |
--- | H6(S) | H2' | --- | 2.9 |
--- | H4 | H3' | --- | 3.0 |
--- | H5 | H1' | --- | 3.5 |
--- | H4 | H1' | --- | 3.9 |
--- | H6(S) | --- | H1” | 3.0 |
--- | H6(S) | --- | NAc | 3.6 |
--- | --- | H4' - H6'(S) | --- | 2.9 |
--- | --- | H2' | H1” | 2.6 |
--- | --- | H1' | H1” | 2.7 |
--- | --- | H2' | H5” | 3.5 |
--- | --- | H1' | NAc | 3.5 |
--- | --- | H3' | H1” | 3.6 |
--- | --- | H6'(S) | NAc | 3.6 |
--- | --- | H2' | H4” | 3.7 |
--- | --- | H1' | H5” | 4.1 |
--- | --- | H2' | NAc | 4.8 |
--- | --- | H4' | NAc | 4.9 |
--- | --- | --- | H5” - H6”(R) | 2.5 |
--- | --- | --- | H5” - H6”(S) | 2.5 |
--- | --- | --- | H4” - H6”(S) | 3.1 |
--- | --- | --- | H2” - NAc | 4.0 |
--- | --- | --- | H1” - NAc | 4.5 |
--- | --- | --- | H3” - NAc | 4.8 |
Only intermolecular and sugar methylene proton NOEs were included to simplify the table. Intramolecular NOEs were used as reference values to calculate the tabulated NOE values.