Table 1.
Normalized peak volumes from 1H-13C HSQC spectra of the four partially 13C-labeled samples.
NMR peak | 0.5:1 sample | 1:1 sample | 2:1 sample | 5:1 sample |
---|---|---|---|---|
1 | 9.9 | 18.0 | 33.7 | 71.4 |
2 | 8.8 | 12.8 | 25.3 | 61.1 |
3 | 11.6 | 17.3 | 32.0 | 70.3 |
4 | 5.2 | 7.5 | 15.4 | 38.6 |
5 | 8.8 | 11.9 | 26.1 | 60.0 |
6 | --- | --- | 10.7 | 30.2 |
7 | 19.9 | 21.5 | 34.7 | 78.3 |