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. Author manuscript; available in PMC: 2008 Feb 1.
Published in final edited form as: J Nat Prod. 2007 Feb 2;70(2):253–258. doi: 10.1021/np060260f

Table 2.

13C NMR data [δ in ppm, mult] of compounds 1, 2 and 4 in CD3OHa and D2Ob

pos. 1a 2b 4c
1 96.14 d 95.05 d 95.6 d
3 153.28 d 152.50 d 153.4 d
4 112.47 s 111.57 s 112.4 s
5 35.21 d 32.40 d 32.5 d
6 31.57 t 29.67 t 30.1 t
7 37.47 t 35.61 t 35.7 t
8 81.66 s 80.37 s 82.8 s
9 46.87 d 45.66 d 45.7 d
10 70.88 t 69.55 t 68.2 t
11 170.74 s 171.25 s 172 s
1′ 100.88 d 98.88 d 99.4 d
2′ 74.62 d 72.72 d 73.3 d
3′ 77.88 d 75.72 d 76.3 d
4′ 71.22 d 70.14 d 70.1 d
5′ 78.40 d 76.38 d 77.0 d
6′ 62.49 t 60.78 d 61.3 d
1″ 169.23 s 169.22 s -
2″ 114.89 d 116.89 d -
3″ 147.03 d 144.32 d -
4″ 127.13 s 127.31 s -
5″, 9″ 131.32 d 131.51 d -
6″, 8″ 116.85 d 115.34 d -
7″ 161.39 s 156.83 s -
a

90 MHz in CD3OD.

b

90 MHz in D2O.

c

75 MHz in D2O; from Jensen, et al. 2002.41