Table 2.
Entry | Ar 1 | Ar 2 | T (°C) | Time (h) | Yield (%) | M.P. (°C) [lit.] |
a | C6H5 | 4-CH3OC6H4 | 28–33 | 1.5 | 96 | 110–112 |
b | C6H5 | 4-CH3C6H4 | 29–33 | 2 | 88 | 128–130 |
c | C6H5 | C6H5 | 32–36 | 2 | 96 | 134–135(134–135) [9] |
d | C6H5 | 4-ClC6H4 | 29–33 | 2 | 86 | 135–136(133–134) [7] |
e | C6H5 | 3-ClC6H4 | 29–33 | 2 | 83 | 134–136 |
f | C6H5 | 2-ClC6H4 | 28–33 | 2 | 85 | 134–135(135–136) [7] |
g | C6H5 | 3-BrC6H4 | 29–33 | 2 | 83 | 141–143 |
h | C6H5 | 4-O2NC6H4 | 28–34 | 3 | trace | |
i | 4-ClC6H4 | C6H5 | 28–33 | 2 | 85 | 143–145 |
j | 3-O2NC6H4 | C6H5 | 28–33 | 3 | trace |
* The preparation of chalcones was referred to [14]