Skip to main content
. 2007 Mar 21;3:13. doi: 10.1186/1860-5397-3-13

Table 2.

Synthesis of 1,3,5-triaryl-2-pyrazolines in the NaAc-HAc aqueous under ultrasound irradiation*

Entry Ar 1 Ar 2 T (°C) Time (h) Yield (%) M.P. (°C) [lit.]

a C6H5 4-CH3OC6H4 28–33 1.5 96 110–112
b C6H5 4-CH3C6H4 29–33 2 88 128–130
c C6H5 C6H5 32–36 2 96 134–135(134–135) [9]
d C6H5 4-ClC6H4 29–33 2 86 135–136(133–134) [7]
e C6H5 3-ClC6H4 29–33 2 83 134–136
f C6H5 2-ClC6H4 28–33 2 85 134–135(135–136) [7]
g C6H5 3-BrC6H4 29–33 2 83 141–143
h C6H5 4-O2NC6H4 28–34 3 trace
i 4-ClC6H4 C6H5 28–33 2 85 143–145
j 3-O2NC6H4 C6H5 28–33 3 trace

* The preparation of chalcones was referred to [14]