Table 3.
Size Analysis of Sulfide-Treated Nanorodsa
t (min) |
count (N) |
length L (nm) |
midsection D1 (nm) |
end width D2 (nm) |
width ratio (D1/D2) |
aspect ratio (L/D1) |
aspect ratio (L/D2) |
---|---|---|---|---|---|---|---|
15 | 95 | 44.3 ± 13 | 11.5 ± 1.5 | 14.5 ± 1.9 | 0.79 ± 0.06 | 3.99 ± 0.83 | 3.17 ± 0.62 |
20 | 103 | 48.9 ± 7.7 | 13.2 ± 1.5 | 16.9 ± 1.6 | 0.80 ± 0.05 | 3.71 ± 0.71 | 2.98 ± 0.47 |
30 | 117 | 50.5 ± 7.5 | 13.7 ± 1.6 | 17.2 ± 1.9 | 0.80 ± 0.04 | 3.71 ± 0.63 | 2.96 ± 0.51 |
40 | 91 | 55.2 ± 11.0 | 18.6 ± 2.5 | 21.1 ± 3.2 | 0.89 ± 0.05 | 2.96 ± 0.65 | 2.63 ± 0.59 |
50 | 103 | 58.1 ± 6.3 | 21.4 ± 2.1 | 24.2 ± 2.5 | 0.89 ± 0.05 | 2.77 ± 0.41 | 2.45 ± 0.37 |
Nanorods were isolated by one C/R cycle in deionized water, prior to TEM sample preparation. Errors represent one standard deviation.