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. Author manuscript; available in PMC: 2007 Apr 27.
Published in final edited form as: J Appl Crystallogr. 2005 Dec;38(6):900–905. doi: 10.1107/S002188980502649X

Table 1. Diffraction data statistics for two thaumatin crystals in the same capillary.

Refined unit-cell parameters were virtually identical in the two crystals, with a = b = 58.6 Å and c = 151.93 Å in P41212. Rint of merging data sets 1 and 2 was 0.04.

Data set 1 Data set 2 Merged
Resolution range (Å) 27.94–1.86 36.34–1.90 36.34–1.86
Number of reflections 20 717 18 350 21 731
Completeness (%) 94.1 99.4 98.7
Completeness, outer (%) 94 99.2 94
Redundancy 7.9 7.3
Initial frame I/σ(I) 9.11 7.94
Final frame I/σ(I) 6.48 5.89
Initial frame I/σouter(I) 2.96 2.64
Final frame I/σouter(I) 1.38 1.28
I/σ(I) 24.07 22.0 30.56
I/σouter(I) 10.69 10.05 10.69
Rsym 0.086 0.094
R 0.145 0.146 0.148
Rfree 0.187 0.195 0.188
Initial frame outer resolution shell (Å) 1.75–1.61 1.75–1.61
Final frame outer resolution shell (Å) 2.10–2.0 1.80–1.69
Number of frames 100 100