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. Author manuscript; available in PMC: 2007 May 14.
Published in final edited form as: J Am Chem Soc. 2006 Jul 26;128(29):9302–9303. doi: 10.1021/ja062637

Table 3.

Reaction Initiation via Aldehyde Alkylation

graphic file with name nihms16459f8.jpg

entry R′ R″ product yield (%)a d.r.b
1 Et Et graphic file with name nihms16459t10.jpg 68 n.a.
2 Ph Et graphic file with name nihms16459t11.jpg 81 1.8:1
3 cyclohexyl Me graphic file with name nihms16459t12.jpg 67 3.5:1
a

Isolated yields.

b

Determined by 1H NMR spectroscopy; the major isomer is shown.