Table 1.
Data collection and refinement statistics
| Wavelength (Å) | 0.979 |
| Resolution range (Å) | 50.0–2.4 (2.48–2.38) |
| Reflections recorded (unique) | 110,313 (24,916) |
| Completeness (%) | 94.1 (92.5) |
| I/ς(I) | 12.7 (3.7) |
| R (I)merge (%)a | 9.6 (30.9) |
| R-factor (2.4 Å)b | 22.8 |
| R-Free (2.4 Å) | 29.4 |
| rmsd for bonds | 0.02 Å |
| rmsd for angles | 2.6° |
| % of residues in allowed Ramachandran regions | 100% (2% in generously allowed) |
a
Rmerge = Σ Σi/Ii − <I>|/Σi |I|, where Ii is an individual intensity measurement and <I> is the average intensity for this reflection, with summation over all data.
b
R-factor = Σ∥Fo| − |FC∥/Σ|FO|.
Values in parentheses refer to statistics for the last shell.