Table 2.

Assigned ¹H and ¹³C chemical shift data for the isolated MPE and mvMPE and for comparison the data for MP and MDE

Group	δ, ppm
	mvMPE		MPE		MDE		MP
	1H	13C	1H	13C	1H	13C	1H	13C
2-CH3	3.814	10.8	3.808	10.7	3.795	10.7	3.815	10.5
31-CH	8.495	130.5	8.489	130.5	8.471	130.3	8.502	130.5
32-CH2z	6.417	117.2	6.414	117.2	6.410	117.2	6.414	117.7
32-CH2e	6.152		6.152		6.165		6.153
5-Meso	10.270	97.2	10.323	97.9	10.313	97.8	10.323	98.0
7-CH3	3.668	10.8	3.793	10.6	3.780	10.8	3.803	10.4
81-CH*	4.166	22.2	8.478	130.5	8.463	130.3	8.483	130.5
81-CH2z†	1.938	16.3	6.409	117.2	6.408	117.2	6.414	117.7
82-CH2e			6.161		6.162		6.153
10-Meso	10.119	96.1	10.244	97.4	10.236	97.1	10.242	97.4
12-CH3	3.693	9.6	3.674	9.7	3.668	9.5	3.702	9.4
131-CH2	4.500	20.8	4.485	21.2	4.457	20.8	4.466	22.4
132-CH2	3.393	36.2	3.388	36.2	3.372	36.1	3.194	40.5
13-OCH3	3.674	49.9	3.674	49.9	3.656	49.9
15-Meso	10.184	96.6	10.157	96.5	10.074	96.1	10.231	97.3
171-CH2	4.454	22.1	4.446	22.1	4.457	20.8	4.466	22.4
172-CH2	3.246	39.2	3.243	39.2	3.372	36.1	3.194	40.5
17-OCH3					3.656	49.9
18-CH3	3.725	9.7	3.719	9.7	3.688	9.5	3.725	9.4
20-Meso	10.227	97.2	10.204	97.1	10.190	97.0	10.201	97.1

Only chemical shifts for ¹³C bearing protons are included, and no attempt was made to assign quaternary carbon. e and z indicate the entgegen and zusammen hydrogens. 

^*For mvMPE, 8¹-CH₂. 

^† For mvMPE, 8²-CH₃.