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. 2007 Apr 22;35(9):3128–3143. doi: 10.1093/nar/gkm169

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© 2007 The Author(s)

This is an Open Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/by-nc/2.0/uk/) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.

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Scheme 1. — Synthetic pathway to 2-iodoadenosine phosphoramidite (ACE® chemistry); (a) HC(OMe)₂NMe₂, DMF, 50°C, 69% (compound 11); (b) TIPS-Cl₂, pyridine, 0°C, 72%.