TABLE 1.
Statistic | Valuea
|
|
---|---|---|
Mg2+ complex | 3′dGTP complex | |
Wavelength (Å) | 1.0 | 1.0 |
Cell parameters (Å) for space group C2221 | ||
a | 160.15 | 163.71 |
b | 180.47 | 180.91 |
c | 57.98 | 58.04 |
Resolution range (Å) | 48-1.85 | 48-2.6 |
No. of observed reflections | 355,151 | 131,992 |
No. of unique reflectionsa | 72,065 (8,212) | 26,929 (3,067) |
Completeness (%) | 99.9 (100) | 99.6 (100) |
Multiplicity | 4.9 (4.9) | 4.9 (4.9) |
Rmergeb | 0.09 (0.540) | 0.10 (0.627) |
I/σ (I) | 14.62 (2.98) | 13.98 (2.54) |
Solvent content (%) | 58.9 | 59.9 |
The numbers in parentheses refer to the last (highest) resolution shell.
Rmerge = ΣhΣi|Ihi − <Ih>|/Σh,iIhi, where Ihi is the ith observation of the reflection h, while <Ih> is its mean intensity.