Table 5.

96-Parallel fluorous Mitsunobu reactions and RapidTrace F-SPE purifications

	1		2		3		4		5		6c		7c		8		9		10		11		12
A	56a	99b	54	99	60	96	60	99	55	98	60	69	50	86	66	99	62	99	59	99	59	99	56	99
B	56	99	54	99	60	96	54	99	55	99	60	82	50	87	57	99	62	99	59	88	59	97	56	99
C	58	99	42	99	36	99	48	99	43	98	36	99	32	96	20	99	51	99	36	99	39	96	42	99
D	43	99	55	99	53	99	55	99	56	99	53	97	45	99	59	99	57	99	53	99	54	97	50	99
E	98	93	69	99	71	94	70	99	63	99	71	99	57	98	79	99	64	99	70	99	68	99	66	99
F	100	99	79	99	75	96	66	99	73	99	75	99	67	99	93	99	61	99	74	99	79	99	70	99
G	58	94	62	95	63	92	63	95	57	91	63	85	52	75	69	97	51	83	46	90	48	94	59	70
H	53	99	58	99	57	99	58	99	59	97	57	94	54	90	64	99	47	99	57	97	57	98	62	99

^ayield%,

^bpurity% by LCMS with UV254 detection,

^cUV230 detection