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. 2005 Apr 22;61(Pt 5):518–520. doi: 10.1107/S1744309105012364

Table 1. Data-collection statistics.

Values in parentheses are for the last resolution shell.

Space group P212121
Crystal system Orthorhombic
Unit-cell parameters (Å) a = 37.2, b = 72.4, c = 138.2
Matthews coefficient (Å3 Da−1) 2.2
Molecules per AU 1
Resolution range (Å) 50–2.4 (2.53–2.4)
Mosaicity (°) 0.66
Total observations 51389
Unique reflections 17229
Completeness (%) 99.7 (100)
Rsym (%) 5.8 (31.3)
Multiplicity 3.4
I/σ(I)〉 (top shell) 18.5 (2.4)

R sym = Inline graphic Inline graphic.