Table 1. Data-collection statistics.
Space group | P212121 |
Crystal system | Orthorhombic |
Unit-cell parameters (Å) | a = 37.2, b = 72.4, c = 138.2 |
Matthews coefficient (Å3 Da−1) | 2.2 |
Molecules per AU | 1 |
Resolution range (Å) | 50–2.4 (2.53–2.4) |
Mosaicity (°) | 0.66 |
Total observations | 51389 |
Unique reflections | 17229 |
Completeness (%) | 99.7 (100) |
Rsym† (%) | 5.8 (31.3) |
Multiplicity | 3.4 |
〈I/σ(I)〉 (top shell) | 18.5 (2.4) |
R sym = .