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. 2004 Oct 16;61(Pt 1):46–48. doi: 10.1107/S1744309104025837

Table 1. Statistical analysis of X-ray diffraction data for native and SeMet complex crystals.

Values in parentheses are for the highest resolution shell.

  Native type II complex SeMet type II complex
X-ray source CHESS (F2 station) NSLS (X8C beamline)
Wavelength (Å) 0.9790 0.9788
Detector CCD CCD
Crystal parameters    
 Space group P212121 P212121
 Unit-cell parameters    
   a (Å) 45.57 45.21
   b (Å) 52.22 52.34
   c (Å) 156.26 154.69
 Resolution (Å) 2.1 (2.18–2.10) 2.0 (2.07–2.00)
 Mosaicity (°) 0.53 0.65
 Solvent content (%) 48 48
 Molecules per AU (heterodimers) 1 1
Data processing    
 No. observed reflections 88650 300975
 No. unique reflections 22173 25648
 Completeness (%) 99.0 (95.8) 99.6 (96.3)
Rsym (%) 5.9 (18.1) 10.3 (35.4)
 Average I/σ(I) 15.8 (4.8) 25.81 (3.0)