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. 2004 Dec 24;61(Pt 1):156–159. doi: 10.1107/S1744309104032762

Table 1. Data-collection statistics.

Values in parentheses are for the highest resolution shell.

Space group C2221
Unit-cell parameters  
a (Å) 60.3
b (Å) 155.04
c (Å) 134.61
 α = β = γ (°) 90.0
Matthews coefficient (Å3 Da−1) 2.7
Solvent content (%) 54.3
No. molecules per AU 2
Resolution range (Å) 30–2.9 (3.0–2.9)
Total reflections 157834
Unique reflections 14399
Redundancy 11.0 (11.1)
I〉/〈σ(I)〉 21.84 (6.94)
Data completeness (%) 99.8 (100.0)
Rsym (%) 10.8 (45.1)

R sym = Inline graphic Inline graphic, where Ih is the integrated intensity of a given reflection and 〈Ih〉 is the average intensity over symmetry equivalents.