Table 1. Data-collection statistics.
Space group | C2221 |
Unit-cell parameters | |
a (Å) | 60.3 |
b (Å) | 155.04 |
c (Å) | 134.61 |
α = β = γ (°) | 90.0 |
Matthews coefficient (Å3 Da−1) | 2.7 |
Solvent content (%) | 54.3 |
No. molecules per AU | 2 |
Resolution range (Å) | 30–2.9 (3.0–2.9) |
Total reflections | 157834 |
Unique reflections | 14399 |
Redundancy | 11.0 (11.1) |
〈I〉/〈σ(I)〉 | 21.84 (6.94) |
Data completeness (%) | 99.8 (100.0) |
Rsym† (%) | 10.8 (45.1) |
R sym = , where Ih is the integrated intensity of a given reflection and 〈Ih〉 is the average intensity over symmetry equivalents.