Table 1. Data-collection statistics and crystal parameters for the different crystal forms of FaeE.
Values in parentheses are for the highest resolution shells.
| FaeE crystal form 2 (data collected from FaeESeMet crystal) | |||||
|---|---|---|---|---|---|
| FaeE crystal form 1 | Absorption edge | Inflection point | High-energy remote | FaeE crystal form 3 | |
| Wavelength (Å) | 0.933 | 0.9789 | 0.9796 | 0.9364 | 0.9364 |
| Resolution range (Å) | 49.8–2.3 (2.4–2.3) | 39.0–2.7 (2.8–2.7) | 39.0–2.7 (2.8–2.7) | 33.0–2.7 (2.8–2.7) | 39.3–2.8 (2.9–2.8) |
| Total reflections | 639018 | 145440 | 140236 | 149032 | 111565 |
| Unique reflections | 122618 (11697) | 19280 (1903) | 19271 (1920) | 19389 (1890) | 18291 (1794) |
| Redundancy | 5.2 (4.0) | 7.5 (7.4) | 7.3 (7.2) | 7.7 (7.4) | 6.1 (6.2) |
| Mosaicity (°) | 0.3 | 0.7 | 0.7 | 0.7 | 1.4 |
| 〈I/σ(I)> | 14.56 (3.7) | 19.5 (5.4) | 19.3 (5.3) | 23.97 (4.9) | 14.91 (7.0) |
| Completeness (%) | 99.5 (95.6) | 98.0 (97.1) | 98.0 (98.2) | 98.6 (96.4) | 99.8 (100.0) |
| Rmerge (%) | 8.3 (39.0) | 7.1 (32.9) | 5.7 (29.9) | 5.3 (40.4) | 12.2 (30.2) |
| Ranom (%) | 3.7 (10.0) | 1.7 (9.9) | 2.6 (13.8) | ||
| Space group | C2 | C2 | C2 | ||
| Unit-cell parameters | |||||
| a (Å) | 195.7 | 136.4 | 109.7 | ||
| b (Å) | 78.5 | 75.7 | 78.6 | ||
| c (Å) | 184.6 | 69.4 | 87.8 | ||
| β (°) | 102.2 | 92.8 | 96.4 | ||
| Beamline | ID14-1 | BW7A | BW7A | ||