Table 1. Data-collection and processing statistics.
Synchrotron radiation | 14-BM-C, APS |
Detector | MAR345 CCD |
Wavelength (Å) | 0.9 |
Space group | P212121 |
Unit-cell parameters (Å) | a = 33.3, b = 35.4, c = 107.4 |
Resolution range (Å) | 20–2.3 |
Unique reflections | 5971 (392) |
Completeness (%) | 98.0 (100.0) |
Redundancy | 6.8 (7.5) |
Rmerge (%) | 7.1 (41.1) |
〈I/σ(I)〉 | 42.9 (8.4) |
Unit-cell volume (Å3) | 126605.3 |
Solvent content (%) | 40.8 |