Table 1. Data-collection parameters and crystallographic data statistics.
Temperature (K) | 110 |
Wavelength (Å) | 1.431 |
Space group | C2 |
Unit-cell parameters (Å, °) | a = 127.97, b = 135.41, c = 75.81, β = 89.95 |
Resolution limits (Å) | 46.6–2.4 (2.53–2.4) |
Total No. of reflections | 297954 |
No. of unique reflections | 48181 |
Completeness (%) | 99.6 (99.7) |
Multiplicity | 6.1 (6.0) |
Rsym (%) | 9.9 (32.5) |
〈I/σ(I)〉 | 17.6 (4.3) |