Table 2.
A: Stability as Concentrated Solutions in 0.1 M acetic acid at 4°C | |||||||
---|---|---|---|---|---|---|---|
Haloperidol | Risperidone | ||||||
Time (weeks) | Concentration (mg/ml) | SD | R.S.D. (%) | Time (weeks) | Concentration (mg/ml) | SD | RSD. (%) |
0 | 4.7 | 0.03 | 0.70 | 0 | 5.6 | 0.08 | 1.33 |
1 | 4.9 | 0.04 | 0.71 | 1 | 5.4 | 0.08 | 1.40 |
2 | 4.9 | 0.16 | 3.24 | 2 | 5.5 | 0.06 | 1.06 |
4 | 4.8 | 0.01 | 2.20 | 4 | 5.7 | 0.19 | 3.28 |
B: Stability of Dilutions in Rodent Drinking Water | |||||||
Haloperidol (Tap water) | Haloperidol (distilled/deionized Water) | ||||||
Time (hours) | Concentration (μg/ml) | SD | R.S.D. (%) | Time (hours) | Concentration (μg/ml) | SD | RSD. (%) |
0 | 20.1 | 0.26 | 1.31 | 0 | 20.5 | 0.22 | 1.06 |
6 | 20.1 | 0.16 | 0.81 | 6 | 20.4 | 0.09 | 0.44 |
24 | 19.7 | 0.11 | 0.57 | 24 | 19.9 | 0.13 | 0.68 |
48 | 19.6 | 0.30 | 1.50 | 48 | 20.0 | 0.03 | 0.16 |
72 | 20.3 | 0.10 | 0.48 | 72 | 20.5 | 0.02 | 0.11 |
96 | 20.1 | 0.07 | 0.34 | 96 | 20.5 | 0.09 | 0.44 |
Risperidone (Tap water) | Risperidone (distilled/deionized Water) | ||||||
0 | 22.2 | 0.33 | 1.47 | 0 | 22.8 | 0.04 | 0.18 |
6 | 22.5 | 0.27 | 1.19 | 6 | 22.8 | 0.22 | 0.95 |
24 | 22.1 | 0.08 | 0.34 | 24 | 22.2 | 0.15 | 0.68 |
48 | 22.5 | 0.36 | 1.59 | 48 | 22.3 | 0.02 | 0.08 |
72 | 22.6 | 0.16 | 0.70 | 72 | 22.3 | 0.39 | 1.73 |
96 | 22.6 | 0.22 | 0.07 | 96 | 22.7 | 0.22 | 0.98 |
N=3 samples per determination; SD= Standard Deviation; RSD= relative standard deviation