Table 1. X-ray diffraction data of human Rad.
Statistics for the outer resolution shell are given in parentheses.
| Beamline | SPring-8/BL41XU |
| Detector | ADSC Quantum 315 CCD |
| Wavelength (Å) | 1.00 |
| Temperature (K) | 100 |
| Oscillation range (°) | 180 (1.5° × 120 images) |
| Exposure time (s) | 30 |
| Space group | P21 |
| Unit-cell parameters (Å, °) | a = 52.2, b = 58.6, c = 53.4, β = 97.9 |
| Resolution (Å) | 50–1.80 (1.86–1.80) |
| Total reflections | 97986 |
| Unique reflections | 28220 |
| Completeness (%) | 94.6 (72.2) |
| Mosaicity | 0.3–0.5 |
| 〈I/σ(I)〉 | 12.4 (2.2) |
| Rmerge† (%) | 6.6 (44.4) |
R
merge =
, where I
i is the observed intensity and 〈I
i〉 is the average intensity over symmetry-equivalent measurements.