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. 2005 Nov 12;61(Pt 12):1049–1053. doi: 10.1107/S1744309105035888

Table 1. X-ray diffraction data and refinement statistics.

Values in parentheses are for the highest resolution shell.

  Edited 10 × 10 Unedited 10 × 10 Edited 23 × 19
Data collection      
 Space group H3 H3 P41212 or P43212
 Unit-cell parameters (Å) a = 39.5, c = 246.4 a = 49.0, c = 235.8 a = 62.5, c = 63.6
 Resolution 29.92–1.35 (1.40–1.35) 23.38–2.85 (2.95–2.85) 36.29–2.80 (2.90–2.80)
 Total reflections 122008 16052 16572
 Unique reflections 30558 4798 3307
 Redundancy 3.99 (1.78) 3.35 (3.67) 5.01 (4.82)
 Completeness (%) 96.8 (77.4) 97.2 (99.8) 97.0 (92.7)
 〈I/σ(I)〉 13.1 (2.2) 10.3 (1.9) 11.4 (2.2)
Rsym (%) 6.3 (35.4) 6.1 (37.9) 9.9 (33.4)
 Twinning fraction 0.38 0.41 None
Refinement statistics      
 Resolution 30.0–1.5    
 No. of atoms (RNA/water) 1257/26    
Rwork/Rfree§ (%) 31.9/31.8    
 R.m.s.d. bonds (Å) 0.0038    
 R.m.s.d. angles (°) 0.94    

R sym = Inline graphic Inline graphic × 100.

R work = Inline graphic Inline graphic × 100. R work was calculated using 93% of the data.

§

R free is defined as the R work calculated using 7% of the data selected randomly and excluded from the refinement.