Skip to main content
. 2005 Nov 24;61(Pt 12):1087–1089. doi: 10.1107/S1744309105037681

Table 1. Crystal parameters, data-collection and refinement statistics.

Values in parentheses are for the highest resolution shell (native, 2.59–2.50 Å; SeMet, 3.63–3.50 Å).

    SeMet
  Native Inflection Peak Remote
Crystal parameters        
 Space group C2221 C2221
 Unit-cell parameters
   a (Å) 58.2 58.1
   b (Å) 95.9 96.0
   c (Å) 167.5 167.2
 No. of molecules in ASU 1 1
Data collection
 X-ray source and detector BNL (X25)/ADSC Q315 CCD
 Resolution (Å) 2.5 3.5    
 Total observations 109448 38377 38181 37311
 Unique reflections 16710 6213 6259 6181
 Completeness (%) 97.8 (99.8) 98.4 (93.3) 98.2 (91.9) 98.3 (92.3)
 Redundancy 6.7 (6.7) 6.3 (6.0) 6.2 (5.7) 6.1 (5.6)
Rsym 0.071 (0.29) 0.059 (0.09) 0.065 (0.10) 0.050 (0.07)
 〈I/σ(I)〉 21.30 (5.4) 30.2 (18.3) 30.7 (17.5) 20.5 (12.1)

R sym = Inline graphic.