Table 1. Data-collection statistics.
The values in parentheses are for the highest resolution bin (approximate interval 0.1 Å).
| Temperature (K) | 100 |
| X-ray source | APS, BioCars 14-BM-C |
| Detector | Quantum 4 CCD |
| Space group | C222 |
| Unit-cell parameters (Å) | a = 188.6, b = 312.0, c = 104.1 |
| Resolution (Å) | 2.4 |
| Total No. of observations | 439493 |
| No. of unique observations | 115857 |
| Multiplicity | 3.8 |
| Data completeness (%) | 97.1 (93.0) |
| No. of data > 2σ(I) | 91071 (4632) |
| 〈I/σ(I)〉 | 17.9 (2.1) |
| Rmerge (%)† | 8.1 (57.7) |
R
merge =
.