Table 1. Data-collection statistics.
X-ray source | I711 |
Wavelength (Å) | 1.029 |
Resolution (Å) | 25.0–2.7 |
Space group | P21 |
Unit-cell parameters | a = 68.1, b = 65.2, c = 101.9, α = 90, β = 102.4, γ = 90 |
Total No. of unique reflections | 22481 |
No. of observed reflections | 82092 |
Completeness (%) | 91.8 (51.4) |
Rmerge† | 4.9 (31.5) |
〈I/σ(I)〉 | 20.2 (2.4) |
Mosaicity (°) | 0.77 |
R merge = , where I hkl(j) is the observed intensity and I hkl is the average value of the intensity.