Table 1.
Data collection statistics | |
Space group | C2 |
Unit cell | a = 185.4 Å, b = 69.3 Å, c = 88.2 Å |
α =90°, β =112.76°, γ = 90° | |
Resolution, Å | 28.5–2.7 |
Outer resolution shell, Å | 2.77–2.70 |
No. of observations | 90,579 |
Unique reflections | 26,015 |
Completeness, % | 90.6 (58.1) |
Rsym, % | 8.7 (54.3) |
Refinement statistics | |
Refinement range, Å | 28.5–2.70 |
Data cutoff (|F|) | 0.0 |
No. of reflections (work/test) | 23,400/2,559 |
Rwork (Rfree), % | 20.4 (25.3) |
rmsd bond lengths, Å | 0.005 |
rmsd bond angles, ° | 0.91 |
Ramachandran statistics, % (favored/allowed/outlier)* | 96.5/3.4/0.1 |
*Determined with RAMPAGE (28).