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. 2007 Sep 19;104(39):15358–15363. doi: 10.1073/pnas.0707406104

Table 1.

Data collection and refinement statistics

Data collection statistics
    Space group C2
    Unit cell a = 185.4 Å, b = 69.3 Å, c = 88.2 Å
α =90°, β =112.76°, γ = 90°
    Resolution, Å 28.5–2.7
    Outer resolution shell, Å 2.77–2.70
    No. of observations 90,579
    Unique reflections 26,015
    Completeness, % 90.6 (58.1)
    Rsym, % 8.7 (54.3)
Refinement statistics
    Refinement range, Å 28.5–2.70
    Data cutoff (|F|) 0.0
    No. of reflections (work/test) 23,400/2,559
    Rwork (Rfree), % 20.4 (25.3)
    rmsd bond lengths, Å 0.005
    rmsd bond angles, ° 0.91
    Ramachandran statistics, %     (favored/allowed/outlier)* 96.5/3.4/0.1

*Determined with RAMPAGE (28).