Table 1.
Data collection and refinement statistics
| Data collection statistics | |
| Space group | C2 |
| Unit cell | a = 185.4 Å, b = 69.3 Å, c = 88.2 Å |
| α =90°, β =112.76°, γ = 90° | |
| Resolution, Å | 28.5–2.7 |
| Outer resolution shell, Å | 2.77–2.70 |
| No. of observations | 90,579 |
| Unique reflections | 26,015 |
| Completeness, % | 90.6 (58.1) |
| Rsym, % | 8.7 (54.3) |
| Refinement statistics | |
| Refinement range, Å | 28.5–2.70 |
| Data cutoff (|F|) | 0.0 |
| No. of reflections (work/test) | 23,400/2,559 |
| Rwork (Rfree), % | 20.4 (25.3) |
| rmsd bond lengths, Å | 0.005 |
| rmsd bond angles, ° | 0.91 |
| Ramachandran statistics, % (favored/allowed/outlier)* | 96.5/3.4/0.1 |
*Determined with RAMPAGE (28).