2 |
3.26 (1H, dq, J = 10.0, 6.8 Hz) |
3.26 (1H, m) |
3 |
5.59 (1H, dd, J = 14.0, 10.0) |
5.59 (1H, m) H3, H10 & H23 overlap
|
4 |
6.20 (1H, dd, J = 14.0, 10.6) |
6.20 (1H, m) H4 and H5 overlap
|
5 |
6.16 (1H, dd, J = 14.5, 10.6) |
6.16 (1H, m) H4 and H5 overlap
|
6 |
5.53 (1H, dd, J = 14.5, 8.5) |
5.53 (1H, dd, J = 14.8, 8.8) |
7 |
3.88 (1H, t, J = 8.5) |
3.89 (1H, t, J = 8.8) |
8 |
3.95 (1H, t, J = 8.5) |
3.95 (1H, t, J = 8.4) |
9 |
5.27 (1H, dd, J = 15.6, 8.5) |
5.27 (1H, dd, J = 14.4, 7.6) |
10 |
5.64 (1H, m) |
5.64 (1H, m) H3, H10 & H23 overlap
|
11a |
2.23 (1H, m) |
2.23 (1H, m) |
11b |
1.82 (1H, m) |
1.82 (1H, m) |
12a |
1.76 (1H, m) |
1.76 (1H, m) |
12b |
1.48 (1H, m) |
1.48 (1H, m) |
13 |
3.41 (1H, m) |
3.40 (1H, m) |
14a |
1.40 (1H, m) |
1.40 (1H, m) |
14b |
1.25 (1H, m) |
1.25 (1H, m) |
15a |
1.58 (1H, m) |
1.58 (1H, m) overlapping w/water
|
15b |
1.33 (1H, m) |
1.33 (1H, m) |
16 |
3.56 (1H, dt, J = 7.5, 7.1) |
3.56 (1H, m) |
17 |
3.72 (1H, dt, J = 7.5, 4.5) |
3.72 (1H, m) |
18 |
4.66 (1H, d, J = 8.3) |
4.66 (1H, d, J = 9.2) |
19 |
2.25 (1H, m) |
2.25 (1H, m) |
20a |
2.40 (1H, d, J = 13.4) |
2.40 (1H, d, J = 14.0) |
20b |
1.79 (1H, m) |
1.79 (1H, m) |
22 |
6.05 (1H, d, J = 15.9) |
6.05 (1H, d, J = 15.2) |
23 |
5.71 (1H, dt, J = 15.9, 6.8) |
5.71 (1H, m) H3, H10 & H23 overlap
|
24 |
2.78 (2H, br d, J = 6.8) |
2.78 (2H, m) |
26a |
4.75 (1H, s) |
4.75 (1H, s) |
26b |
4.71 (1H, s) |
4.71 (1H, s) |
27 |
1.72 (3H, s) |
1.72 (3H, s) |
28a |
4.98 (1H, s) |
4.98 (1H, s) |
28b |
4.87 (1H, s) |
4.87 (1H, s) |
29 |
0.92 (3H, d, J = 6.6) |
0.92 (3H, d, J = 6.8) |
30 |
1.25 (3H, d, J = 6.8) |
1.25 (3H, d, J = 6.8) |