Table 5.
Sample | Volume | Total Protein | Total Activity | Recovery | Specific Activity | Fold-purification |
---|---|---|---|---|---|---|
mL | mg | μmol/h | % | μmol/h/mg | ||
Cell-free lysatea | 168 | 3120 | 156 | 100 | 0.05 | 1 |
IMAC wasteb | 740 | 2860 | 1.3 | 1 | 0.0005 | 0.01 |
Cation exchange wastec | 1830 | 15 | 2.4 | 2 | 0.16 | 3.2 |
Purified His7-TEVd | 80 | 395 | 133 | 85 | 0.34 | 6.7 |
The lysate obtained from 25 g of MHT237Δ cells.
Collected as flow-through from sample injection and column wash prior to elution.
Collected as flow-through from sample injection and column wash prior to elution.
Pooled sample obtained after four cycles of the 2-step automated purification.