Figure 2.
Assignment of proton, nitrogen and carbon resonances of TAR/LR06(GA)complex. (A) Imino proton region of the 1D spectrum (top) and the 1H/15N HSQC spectrum (bottom). (B) H6/8-H1′ region of a NOESY spectrum recorded at 15°C in 100% D2O with a mixing time of 200 ms. Dashed lines represent sequential assignment of H6/8-H1′. (C) 1H-13C HSQC spectrum showing the aromatic H8-C8, H6-C6 and H2-C2 correlations of TAR 13C-15N labelled complexed with LR06(GA).