Table 1.
Carbon no. | 13C | 1H |
---|---|---|
1 | 45.4 s | |
2 | 50.0 d | 2.50 (bt, J 9.0) |
3 | 20.2 t | 1.90, 1.69 |
4 | 28.5 t | 1.51 |
5 | 39.3 t | 1.80, 1.70 |
6 | 62.1 t | 4.09 (t, J 7.5) |
7 | 23.3 t | 1.70, 1.39 |
8 | 40.6 t | 1.39, 1.28 |
9 | 32.5 t | 1.90 |
10 | 146.2 s | |
11 | 111.2 t | 4.80 (bs) |
12 | 23.1 q | 1.66 (bs) |
13 | 145.6 s | |
14 | 111.6 t | 4.89 (bs), 4.79 (bs) |
15 | 24.6 q | 1.57 (bs) |
16 | 170.8 s | |
17 | 21.3 q | 1.69 (s) |
600 and 100.5 MHz, C6D6, coupling constants (J) are expressedin Hz.