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Electrochemical comparisons. (a) Cyclic and differential pulse voltamograms of [FeIV(O)(TMC)(NCCH3)]2+ (1-NCCH3) in CH3CN at 25°C (Left) and [FeIV(O)(TMCS)]+ (1′-SR) in 1:1 CH3OH/CH3CN at −30°C (Right). (b) Plot of log k2 determined in the oxidation of DHA at 0°C against Ep,c values of [FeIV(O)(TMC)(X)]n+ complexes and [FeIV(O)(TMCS)]+ in 1:1 CH3CN/CH3OH measured at −30°C.
