Table 2.
Data Collection and Refinement Statistics
| apoPPT |
PPT + CoA |
PPT + ACP + CoA |
|
|---|---|---|---|
| PDB ID | 2BYD | 2C43 | 2CG5 |
| Space group | P212121 | P212121 | P3221 |
| Unit cell | a = 63.78 Å, b = 69.95 Å, c = 71.24 Å | a = 65.59 Å, b = 68.96 Å, c = 70.75 Å | a = b = 69.36 Å, c = 184.7 Å |
| No. of unique reflection | 21391 | 19791 | 14864 |
| Resolution | 47.5–2.00 (2.10–2.00) | 32.8–1.93 (2.02–1.93) | 34.7–2.70 (2.80–2.70) |
| Completeness (%) | 96.4 (77.6) | 80.3 (29.2) | 99.9 (100) |
| Redundancy | 6.6 (4.0) | 5.0 (0.7) | 10.4 (10.6) |
| I/σ | 11.8 (2.23) | 16.5 (3.59) | 17.9 (3.35) |
| Rint | 0.128 (0.578) | 0.084 (0.245) | 0.090 (0.582) |
| Rcryst/Rfree | 0.176/0.242 | 0.161/0.219 | 0.195/0.247 |
| Rmsd bond length (Å) | 0.010 | 0.017 | 0.013 |
| Rmsd bond angle (°) | 1.28 | 1.66 | 1.50 |
| No. protein atoms | 2315 | 2276 | 2638 |
| No. hetero atoms, ions | 9 | 50 | 46 |
| No. water molecules | 189 | 180 | 24 |
Highest resolution shell indicated in parentheses.