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. Author manuscript; available in PMC: 2008 Oct 10.
Published in final edited form as: Polyhedron. 2007 Oct 10;26(16):4664–4672. doi: 10.1016/j.poly.2007.03.048

Table 1.

Crystallographic Details for [Fe(OEP)(NO3)] and [Fe(TPP)(NO3)]

[Fe(OEP)(NO3)] [Fe(TPP)(NO3)]
formula C36H44FeN5O3 C44H28FeN5O3
FW, amu 650.61 730.56
a, Å 13.209(3) 10.0271(3)
b, Å 13.774(3) 16.1341(5)
c, Å 19.258(4) 16.1341(5)
β, deg 105.50(3) 90.330(2)
γ, deg 90 90.330(2)
V, Å3 3376.2(12) 3399.24(17)
space group P21/c P21/n
Z 4 4
μ, mm−1 0.489 0.495
radiation MoKα, λ̄ = 0.71073 Å MoKα, λ̄ = 0.71073 Å
temperature, K 293 100(2)
final R indices [I > 2σ (I)] R1 = 0.0502, wR2 = 0.1140 R1 = 0.0447, wR2 = 0.1167
final R indices (all data) R1 = 0.0802, wR2 = 0.1311 R1 = 0.0704, wR2 = 0.1405