Table 1. Data-collection and processing statistics.
Values in parentheses are for the last shell.
| Space group | P21212 |
| Radiation | BL41XU, SPring-8 |
| Unit-cell parameters (Å) | a = 225.3, b = 123.3, c = 91.3 |
| Temperature (K) | 100 |
| Wavelength (Å) | 1.0 |
| Oscillation range (°) | 1.0 |
| Distance (mm) | 435 |
| No. of frames | 120 |
| Resolution limit (Å) | 50.0–3.2 (3.31–3.20) |
| Total reflections | 197722 (17898) |
| Independent reflections | 42642 (4073) |
| Average redundancy | 4.5 (4.4) |
| Average I/σ(I) | 5.5(3.3) |
| Completeness (%) | 99.4 (97.0) |
| Rmerge† | 0.112 (0.522) |
†
R
merge = 
, where I(hkl)j is the jth measurement of the intensity of reflection hkl and 〈I(hkl)〉 is the mean intensity of reflection hkl.