Table 1. Data-collection and data-processing parameters.
Space group | P41 |
Unit-cell parameters (Å) | a = b = 47.94, c = 50.2 |
Oscillation range (°) | 1.0 |
Resolution (Å) | 2.93 (3.03–2.93) |
No. of molecules per ASU | 2 |
Matthews coefficient VM (Å3 Da−1) | 1.99 |
Solvent content (%) | 37.0 |
No. of observations | 8576 |
No. of unique reflections | 2276 |
Mosaicity | 0.38 |
Completeness (%) | 95.2 (89.8) |
Rmerge† (%) | 10.8 (24.2) |
I/σ(I) for highest shell | 2.1 |
R merge = , where I(h)i is the observed intensity of the ith measurement of reflection h and I(h) is the mean intensity of reflection h calculated after scaling.