Table 1. X-ray data-collection statistics.
Values in parentheses refer to the highest resolution shell.
| Inflection | Peak | Remote | |
|---|---|---|---|
| Wavelength (Å) | 0.9792 | 0.9800 | 0.9776 |
| Space group | P212121 | ||
| Resolution (Å) | 20.0–2.35 (2.39–2.35) | 20.0–2.35 (2.39–2.35) | 20.0–2.35 (2.39–2.35) |
| Unit-cell parameters (Å) | a = 50.97, b = 60.74, c = 136.54 | ||
| No. of observations | 124573 (4543) | 125245 (4570) | 113108 (4165) |
| Unique reflections | 17975 (826) | 18004 (831) | 18036 (850) |
| Completeness (%) | 99.3 (93.2) | 99.5 (93.8) | 99.7 (95.9) |
| Rmerge† (%) | 7.7 (41.4) | 9.3 (43.4) | 8.4 (42.7) |
| Average I/σ(I) | 23.13 (3.54) | 19.72 (3.44) | 21.87 (3.36) |
| Redundancy | 6.9 (5.5) | 7.0 (5.5) | 6.3 (4.9) |
| Mosaicity | 0.75 | 0.75 | 0.70 |
| Monomers per ASU | 1 | ||
†
R
merge = 
, where I(h) is the observed intensity and 〈I(h)〉 is the mean intensity of reflection h over all measurements of I(h).