Table 1. Summary of the data statistics.
Values in parentheses indicate the statistics for the highest resolution shell.
| Native | Pt derivative | Os derivative | |
|---|---|---|---|
| Space group | P21 | P21 | P21 |
| Unit-cell parameters (Å, °) | a = 48.16, b = 72.75, c = 125.74, β = 94.13 | a = 47.68, b = 72.85, c = 126.39, β = 94.04 | a = 47.90, b = 72.86, c = 126.46, β = 93.17 |
| Wavelength (Å) | 1.0000 | 1.0718 | 1.1399 |
| Resolution range (Å) | 2.4 (2.53–2.4) | 2.8 (2.95–2.8) | 2.8 (2.95–2.8) |
| Observations | 128271 (17594) | 81089 (11863) | 77487 (11489) |
| Unique reflections | 33960 (4885) | 21398 (3069) | 21515 (3108) |
| Completeness (%) | 99.6 (98.8) | 99.7 (99.9) | 99.6 (100.0) |
| Redundancy | 3.8 (3.6) | 3.8 (3.9) | 3.6 (3.7) |
| Mean (I)/sd(I) | 16.7 (4.9) | 12.4 (2.6) | 16.3 (4.7) |
| I/σ(I) | 5.1 (3.1) | 5.8 (1.9) | 4.5 (2.6) |
| Rsym (%) | 6.8 (23.8) | 7.0 (37.9) | 6.4 (24.9) |
| Rano (%) | 7.6 (26.3) | 6.1 (15.0) |