Table 1. Crystallographic statistics.
The X-ray data were processed using HKL-2000 (Otwinowski & Minor, 2001 ▶). Values in parentheses are for the highest resolution bin.
PDB code | 2i5d |
Space group | P21212 |
Unit-cell parameters (Å) | a = 31.1, b = 105.0, c = 49.9 |
Z (No. of molecules per ASU) | 1 |
VM (Å3 Da−1) | 1.89 |
Solvent content† (%) | 34.96 |
Resolution range (Å) | 105–1.63 (1.69–1.63) |
No. of observed/unique reflections | 123793/20838 |
Completeness (%) | 98.1 (98.2) |
Multiplicity | 5.9 (5.3) |
Rsym‡ (%) | 4.8 (44.2) |
I/σ(I) | 35.7 (3.3) |
Rcryst | 19.0 |
Rfree§ | 24.0 |
No. of atoms | 1888 |
No. of water atoms | 228 |
R.m.s.d. bonds (Å) | 0.013 |
R.m.s.d. angles (°) | 1.39 |
Ramachandran analysis¶ (%) | |
Residues in most favorable region | 98.2 |
Residues in allowed regions | 1.2 |
Residues in disallowed regions | 0.6 |
Average B (Å2) | 20.8 |