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. 2006 Nov 30;62(Pt 12):1239–1242. doi: 10.1107/S1744309106046367

Table 1. Data-collection statistics.

Values in parentheses are for the highest resolution shell.

  Crystal form I Crystal form II
Detector MAR CCD MAR CCD
Beamline BW7A X13
Data-collection temperature (K) 100 100
Wavelength (Å) 0.9150 0.8073
Unit-cell parameters (Å) a = b = 74.70, c = 78.97 a = 44.26, b = 81.99, c = 140.89
Space group P31 or P32 P212121
Content of the asymmetric unit 2 monomers 2 monomers
Resolution range (Å) 15.0–2.60 (2.69–2.60) 20–1.70 (1.76–1.70)
No. of observed reflections 178588 (20260) 318867 (22384)
No. of unique reflections 15027 (1809) 51851 (5596)
Rmerge 0.110 (0.763) 0.065 (0.165)
Completeness 100 (100) 90.4 (82.2)
I/σ(I) 24.38 (2.27) 17.35 (6.13)
Redundancy 11.88 (11.20) 6.15 (4.00)

R merge = Inline graphic Inline graphic.