Table 1. Data-collection statistics.
Crystal form I | Crystal form II | |
---|---|---|
Detector | MAR CCD | MAR CCD |
Beamline | BW7A | X13 |
Data-collection temperature (K) | 100 | 100 |
Wavelength (Å) | 0.9150 | 0.8073 |
Unit-cell parameters (Å) | a = b = 74.70, c = 78.97 | a = 44.26, b = 81.99, c = 140.89 |
Space group | P31 or P32 | P212121 |
Content of the asymmetric unit | 2 monomers | 2 monomers |
Resolution range (Å) | 15.0–2.60 (2.69–2.60) | 20–1.70 (1.76–1.70) |
No. of observed reflections | 178588 (20260) | 318867 (22384) |
No. of unique reflections | 15027 (1809) | 51851 (5596) |
Rmerge† | 0.110 (0.763) | 0.065 (0.165) |
Completeness | 100 (100) | 90.4 (82.2) |
I/σ(I) | 24.38 (2.27) | 17.35 (6.13) |
Redundancy | 11.88 (11.20) | 6.15 (4.00) |
R merge = .