Table 1.
Crystallographic Data and Refinement Statistics
| Data Collection | SOCS4-ElonginC-ElonginB | ||
|---|---|---|---|
| Space group | H3 | ||
| Cell dimensions (Å) | a = 154.770, b = 154.770, c = 67.909 | ||
| Resolution (Å) | 2.55 | ||
| Total obs. (unique, red.) | 56643 (19724, 2.71) | ||
| Completeness (outer shella) | 99.7% (97.9%) | ||
| Rmerge (outer shella) | 0.13 (0.48) | ||
| I/σ (outer shella) | 9.14 (2.0) | ||
| Refinement | |||
| Rwork (Rfreeb) (%) | 17.4 (22.3) | ||
| Protein atoms (water) | 2806 (113) | ||
| Hetero groups: | ethylene glycol, Na+, Cl− | ||
| Rmsd bond length (Å) | 0.013 | ||
| Rmsd bond angle (o) | 1.438 | ||
| Average B Factor (Å2) | |||
| Protein atoms | 29.8 (SOCS4) 34.2 (El.B) 32.1 (El.C) | ||
| Solvent atoms | 26.1 | ||
| Other | 53.7 | ||
| Ramachandran | SOCS4 | ElonginB | ElonginC |
| Allowed (%) | 100 | 96.7 | 100 |
| Generously allowed (%) | 0 | 2.2 | 0 |
| Dissallowed (%) | 0 | 1.1 | 0 |
a
Outer shell 2.65–2.55 Å.
b
Using randomly selected 5% of data.