Table 2.

Crystallographic refinement, high-salt form

Space group	P212121
Cell dimensions, Å	a = 58.1, b = 105.2,  c = 154.2
Observations, 25–2.5 Å
Total	482,448
Unique	30,451
Completeness, %
Total	91.1
Last shell	86.0
Rsym, %
Total	7.1
Last shell	26.2
R factor (Rfree), %	20.9 (27.1)
rms deviation in bond lengths, Å	0.008
rms deviation in bond angles, °	1.5
No. of nonhydrogen atoms
Protein	6,328
Water	339