Table 1. Data-collection statistics.
Crystal | Apo-GpdQ | Zn-GpdQ | Co-GpdQ |
---|---|---|---|
Space group | P213 | P213 | P213 |
Unit-cell parameter a (Å) | 164.13 | 164.26 | 164.46 |
Temperature (K) | 100 | 100 | 100 |
Wavelength (Å) | 0.97929 | 1.28269 | 0.97929 |
Resolution (Å) | 50–3.0 (3.19–3.0) | 50–2.9 (3.08–2.9) | 50–3.0 (3.19–3.0) |
Unique reflections | 29709 | 32293 | 29959 |
Redundancy | 6.8 (6.4) | 12.5 (11.2) | 14.0 (12.3) |
〈I/σ(I)〉 | 19.7 (2.8) | 32.2 (4.6) | 34.3 (4.6) |
Completeness | 99.9 (99.9) | 100 (100) | 100 (100) |
Rsym (%) | 11.2 (50.7) | 7.7 (43.6) | 7.3 (42.4) |